By Martin D. Kamen (auth.), Seymour Rothchild (eds.)
Advances in Tracer technique, quantity 2, files the professional ceedings of the sixth, seventh, and eighth Symposia on Advances in Tracer method. those Symposia, that are a part of a continual sequence subsidized by way of the hot England Nuclear Corp. and the Packard tool corporation, Inc., are dedicated to the whole isotope tracer box: education and research of categorized compounds, purposes within the chemical, biochemical, and medical fields, and overall healthiness physics issues linked to tracer paintings. The papers during this quantity mirror convinced developments which might be famous within the tracer box: expanding reliance on biochemical tools for labeling esoteric compounds, transforming into understanding of the issues of radiation decomposition, using complicated instrumentation for the research and detection of radioactive substrates, and the quickly growing to be program of tracer compounds to medical prognosis. the 3 Symposia at which the papers have been awarded have been hung on the next dates: DATE place CHAIRMAN 11/16/62 ny urban Daniel Steinberg, leader Laboratory of Ce1lular body structure and Metabolism, nationwide center Institute, Bethesda, Maryland 3/8/63 la Martin Kamen college of California San Diego, California 11/8/63 Chicago Joseph L. Rabinowitz Veterans management medical institution Philadelphia, Pennsylvania once more, it's the editor's excitement to recognize the aid of his colleagues in making plans and working a few of the Symposia, in addition to the superb cooperation of the chairmen, who acquitted themselves of their appointed initiatives in a most productive demeanour, With humor and figuring out. S. R. Boston, Mass.
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Extra resources for Advances in Tracer Methodology: Volume 2 A collection of papers presented at the Sixth, Seventh, and Eight Symposia on Tracer Methodology plus other papers selected by the editor
Trav. Chim. 73:161 (1954). Stoll, A.. , and Renz, J .. He1v. Chim. Acta. 39:993 (1956). Wilzbach, K. , J. Am. Chern. Soc. 79:1013 (1957). BIOSYNTHESIS OF LABELED CARBOHYDRATES AND OTHER COMPOUNDS OF BIOCHEMICAL INTEREST* S. Abraham Department of Physiology University of California Berkeley. California With the availability of purified enzymes and enzyme systems, a great variety of C14_ and H3-labeled compounds of biological interest can now be prepared with relative ease. The advantages of the use of these biological methods for the synthesis of labeled compounds are obvious when one considers the difficulties involved in preparing a compound through a long series of organic reactions.
L. Bastin, and B. E. Gordon 43 Separation Procedure The product from a carbene insertion reaction is 65 ml of a 2-3% solution of insertion products (.... 1 g) in the original substrate. To isolate the various insertion products in high purity from this solution by distillation would require distillation columns of extremely high efficiency. Preparative-scale gas chromatography is well suited to such separations and was therefore used. The purified products were isolated with a trapping efficiency of about 90%.
J. Am. Chem. Soc. 78:3224 (1956). , Richardson, D. , and Durrett, L. , Anal. Chem. 5 (1963). Farley, F. F .. and Gordon, B. , 1959 Fifth World Petroleum Congress, New York, Section X, Paper 5. International Atomic Energy Agency, Symposium on the Chemical Effects of Nuclear Transformations, Vol. II, Prague, October 1960, pp. 3-145. Kirmse, W.. Angew. Chem. 73:161 (1961). Lange, N. A.. , Handbook Publishers, Sandusky, Ohio (1946). M .. , J. Am. Chem. Soc. 81:106 (1959). , Ann. Chem. 604:151 (1957).